반응 #75340

반응 방정식

2-methyl-3-cyanopyridine

DMF

→

N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine

반응 조건

후처리

1. 1
   기타N,N-dimethyl-2-(3-cyano-2-pyridyl)ethenamine was prepared

실험 절차

N,N-dimethyl-2-(3-cyano-2-pyridyl)ethenamine was prepared using the procedure of 4 A from 2-methyl-3-cyanopyridine (9.0 g, 0.076 m), DMF acetal (11.0 g, 0.092 m) and DMF (50 mL) yielding N,N-dimethyl-2-(3-cyano-2-pyridyl) ethenamine b.p.=133°-135° (0.3 mm), m.p.=49°-50° after sublimation at 50° (0.3 mm).

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