반응 #75290

ord-c507f2867afc4396a8193fc0532cd35c

반응 방정식

c1ccncc1
pyridine
O=C(CBr)c1ccccc1
phenacyl bromide
O=C(C[n+]1ccccc1)c1ccccc1.[Br-]
N-phenacylpyridinium bromide

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The slightly exothermic reaction
  2. 2
    기타was accompanied by the precipitation of the solid N-phenacylpyridinium bromide
  3. 3
    여과The salt was then filtered
  4. 4
    세척washed thoroughly with anhydrous ether

실험 절차

N-phenacylpyridinium bromide was prepared by slowly adding phenacyl bromide to a stirred flask containing an equimolar quantity of pyridine. The slightly exothermic reaction was accompanied by the precipitation of the solid N-phenacylpyridinium bromide. The salt was then filtered and washed thoroughly with anhydrous ether.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04175963uspto-grants-1979_11