반응 #75080

반응 방정식

2-bromopropene

2-methyl-3-buten-2-ol

piperidine

triphenylphosphine

→

2,5-dimethyl-6-piperidinohex-4-en-2-ol

수율 80.0%

반응 조건

실험 절차

A mixture of 10 mmoles 2-bromopropene, 12.5 mmoles 2-methyl-3-buten-2-ol, 30 mmoles piperidine, 0.10 mmole palladium acetate and 0.20 mmole triphenylphosphine were heated together at 100° C. for 20 hrs. From the reaction mixture there was isolated an 80% yield of 2,5-dimethyl-6-piperidinohex-4-en-2-ol.

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