반응 #75022
ord-3c2d463041064f17a5965d17a1397be7
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도heated under nitrogen in 300 ml
실험 절차
Octene-1 in an amount of 3.37 g. and 4.8 g. of freshly prepared MnO2.4H2O were mixed with and heated under nitrogen in 300 ml. glacial acetic acid containing 90 g. potassium acetate. After a reaction time of less than two hours, gamma-n-hexyl-butyrolactone was obtained in 74% yield.