반응 #75018
ord-918feb052ddd4aa081fbb6b976105ed8
반응 방정식
potassium propionate
Styrene
→
alpha-methyl-gamma-phenyl butyrolactone
수율 50.0%
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.WAITIn less than an hour
실험 절차
Styrene in an amount of 2.1 grams and 11.65 grams of manganic acetate, Mn(C2H3O2)3.2H2O, comprising two equivalents of Mn+3 based on titration value, were refluxed under nitrogen in 200 milliliters of propionic acid containing 20 grams of potassium propionate. In less than an hour, a 50% yield of alpha-methyl-gamma-phenyl butyrolactone was obtained.