반응 #74910
ord-9afeabfb0de946a896d15fcb22c8c879
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.DISTILLATIONAfter distilling off the solvent under reduced pressure
실험 절차
5 g of 6-chloro-1-tetralone are reacted with 4.4 g of bromine in ethyl acetate analogously to the instructions indicated in Example 29 (a). After distilling off the solvent under reduced pressure, 2-bromo-6-chloro-1-tetralone is obtained as an amorphous residue, which is used without further purification.