반응 #74350

ord-c005bb11a15b440d8c16419d0781d515

반응 방정식

NC(=S)NC1CCCCCC1
N-cycloheptylthiourea
COC(=O)C1(Br)CCCCC1
methyl 1-bromocyclohexanecarboxylate
→
O=C1N=C(NC2CCCCCC2)SC12CCCCC2
2-(Cycloheptylamino)-1-thia-3-azaspiro[4.5]dec-2-en-4-one

반응물

NC(=S)NC1CCCCCC1
N-cycloheptylthiourea
COC(=O)C1(Br)CCCCC1
methyl 1-bromocyclohexanecarboxylate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Synthesis

실험 절차

Synthesis was performed from N-cycloheptylthiourea and methyl 1-bromocyclohexanecarboxylate according to Method D.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08541592B2uspto-grants-2013_09