반응 #74045
ord-b0d4e10ac7aa4208b2090870c6d587c7
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도the mixture was cooled in an ice-water bath
- 2기타After the completion of the reaction
- 3여과the resultant was filtered
- 4기타to obtain a precipitate
- 5건조The precipitate was dried under reduced pressure, whereby 15.4 g of 3-(3-hexadecyl-1-imidazolio)-1-propanesulfonate (M-1)
- 6기타was obtained
실험 절차
12.3 g of N-hexadecylimidazole was dissolved in 80 ml of acetone, and the mixture was cooled in an ice-water bath. Into the resultant, a solution in which 5.13 g of 1,3-propanesultone was dissolved in 80 ml of acetone was dripped, and after the dripping was completed, the resultant was stirred at room temperature. After the completion of the reaction, the resultant was filtered to obtain a precipitate. The precipitate was dried under reduced pressure, whereby 15.4 g of 3-(3-hexadecyl-1-imidazolio)-1-propanesulfonate (M-1) represented by the chemical formula (M-1) was obtained.