반응 #73873

ord-98ecc165e9fa444bb6cf22925aea77b3

반응 조건

온도
180°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    여과filtered

실험 절차

1-(4-Bromo-phenyl)-cyclopropanecarbonitrile (5 g, 22.5 mmol) and potassium hydroxide (5 g, 89.3 mmol) were combined in ethylene glycol (70 mL), and the reaction was stirred at 180° C. for 4 hours. The mixture was poured into H2O, acidified, and filtered to give the title compound.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08541587B2uspto-grants-2013_09