반응 #735845

ord-3087471c89744d09b88571c819c86720

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    여과The mixture was filtered
  2. 2
    농축concentrated by evaporation in vacuo

실험 절차

An amount of 0.60 gm (1.34 m mol) of ethyl 4-[(1-(2-piperidino-phenyl)-1-butyl)-aminocarbonylmethyl]-cinnamate was hydrogenated in 10 ml of ethanol on 0.20 gm of 10% palladium/charcoal at ambient temperature under 5 bar of hydrogen. The mixture was filtered and concentrated by evaporation in vacuo.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04735959uspto-grants-1988_04