반응 #735816

ord-52b9c29010f944428902b785d6ca64f8

반응 방정식

CCOC(=O)c1ccc(C(C(N)=O)C(C)c2ccccc2N2CCCCC2)cc1
4-[(1-(2-piperidino-phenyl)-ethyl)-aminocarbonylmethyl]-benzoic acid ethyl ester
[Al+3].[H-].[H-].[H-].[H-].[Li+]
lithium aluminum hydride
→
CC(c1ccccc1N1CCCCC1)C(C(N)=O)c1ccc(CO)cc1
4-[(1-(2-Piperidino-phenyl)-1-ethyl)-aminocarbonylmethyl]-benzyl alcohol

반응물

CCOC(=O)c1ccc(C(C(N)=O)C(C)c2ccccc2N2CCCCC2)cc1
4-[(1-(2-piperidino-phenyl)-ethyl)-aminocarbonylmethyl]-benzoic acid ethyl ester
[Al+3].[H-].[H-].[H-].[H-].[Li+]
lithium aluminum hydride

시약

없음

용매

C1CCOC1
tetrahydrofuran

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

Prepared from 4-[(1-(2-piperidino-phenyl)-ethyl)-aminocarbonylmethyl]-benzoic acid ethyl ester by lithium aluminum hydride reduction in tetrahydrofuran.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04735959uspto-grants-1988_04