반응 #735814

반응 방정식

hydrogen

4-[(1-(2-piperidino-phenyl)-ethenyl)-aminocarbonylmethyl]-benzoic acid

→

4-[(1-(2-Piperidino-phenyl)-1-ethyl)-aminocarbonylmethyl]-benzoic acid

용매

ethanol

반응 조건

후처리

1. 1
   여과After 1.5 hours the catalyst was filtered off
2. 2
   기타the filtrate was evaporated in vacuo

실험 절차

One hundred milligrams (0.2744 m mol) of 4-[(1-(2-piperidino-phenyl)-ethenyl)-aminocarbonylmethyl]-benzoic acid in 5 ml of absolute ethanol were hydrogenated in the presence of 50 mg of palladium/charcoal (10%) at 20° C. and at a hydrogen pressure of 1 bar under shaking. After 1.5 hours the catalyst was filtered off, and the filtrate was evaporated in vacuo.

출처