반응 #73546

ord-4bb281048f28408e8885ca421d2baf5d

반응 방정식

CC1(C)OCC(CNC2CCCC2)CO1
N-[(2,2-dimethyl-1,3-dioxan-5-yl)methyl]cyclopentanamine
O=S(=O)(Cl)c1ccc(Cl)nc1
6-chloropyridine-3-sulfonyl chloride
NN.O
hydrazine hydrate
→
CC1(C)OCC(CN(C2CCCC2)S(=O)(=O)c2ccc(NN)nc2)CO1
N-cyclopentyl-N-[(2,2-dimethyl-1,3-dioxan-5-yl)methyl]-6-hydrazinylpyridine-3-sulfonamide

반응물

CC1(C)OCC(CNC2CCCC2)CO1
N-[(2,2-dimethyl-1,3-dioxan-5-yl)methyl]cyclopentanamine
O=S(=O)(Cl)c1ccc(Cl)nc1
6-chloropyridine-3-sulfonyl chloride
NN.O
hydrazine hydrate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The compound is prepared

실험 절차

The compound is prepared according to processes 14.1 and 5.2, starting with N-[(2,2-dimethyl-1,3-dioxan-5-yl)methyl]cyclopentanamine, 6-chloropyridine-3-sulfonyl chloride and hydrazine hydrate.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08541455B2uspto-grants-2013_09