반응 #7318
ord-befbfb3aff7c451d95620ddeb9864f61
반응 방정식
trifluoromethanesulfonic anhydride
dimethyl carbonate
→
methyl trifluoromethanesulfonate
수율 197.7%
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
731 g (2.59 mol) of trifluoromethanesulfonic anhydride and 232 g (2.58 mol) of dimethyl carbonate are added to the residue, and the process described above is repeated. 837 g of methyl trifluoromethanesulfonate having a purity of greater than 99% are isolated (yield: 99.1%).