반응 #726534

반응 방정식

2-(1,3-dioxolan-2-yl)-4-methoxy-1-nitrobenzene

sodium acetate

→

2-(1,3-dioxolan-2yl)-4-methoxyphenylamine

용매

ethyl acetate

반응 조건

후처리

1. 1
   여과The reaction mixture was filtered
2. 2
   농축the filtrate was concentrated

실험 절차

A solution of 2-(1,3-dioxolan-2-yl)-4-methoxy-1-nitrobenzene (1eq) in ethyl acetate was treated with sodium acetate (0.08eq) and platinum oxide (0.06eq) and hydrogenated in a Parr apparatus at 50 psi for 16 hours. The reaction mixture was filtered and the filtrate was concentrated to give 2-(1,3-dioxolan-2yl)-4-methoxyphenylamine in quantitative yield.

출처