반응 #723958
ord-c8607af1eb714855bbe19d2842843eca
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반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도The base particles, along with helium gas, were cooled
- 2기타Consequently, a polymerization reaction
실험 절차
The base particles, along with helium gas, were cooled and introduced through the particle intake 4 into the vapor atmosphere of 1,4-butanedisulfonyl chloride in the condensing chamber 26. Next, in the mixing section 22, the vapor of 1,4-butanedisulfonyl chloride was cooled, and the introduced base particles were exposed thereto for 10 minutes. Consequently, a polymerization reaction, using as a catalyst triethylenediamine contained in the base particles, took place on the surface of the base particles between di(2-mercaptoethyl)ether and 1,4-butanedisulfonyl chloride, forming a film of di(2-mercaptoethyl)ether-1,4-butanedisulfonyl chloride co-polymer.