반응 #722492

ord-12c1cd2605a4457da0efd5eea04227ca

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타obtained

실험 절차

In the same manner as in Example 102 except that 3-(2,4,5,6-tetrahydrocyclopentapyrazol-3-yl)propionic acid obtained in Starting Material Synthesis Example 4 and 1-(4-methylphenyl)piperazine were used instead of 3-(4,5,6,7-tetrahydro-2H-indazol-3-yl)propionic acid obtained in Starting Material Synthesis Example 1 and 4-(4-chlorophenyl)piperidine, 3-(3-(4-(4-methylphenyl)piperazin-1-yl)propyl)-2,4,5,6-tetrahydrocyclopentapyrazole was obtained, m.p. 101-102° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06187774B1uspto-grants-2001_02