반응 #71574

반응 방정식

1,4-dithiane

tetrahydrofuran

methyltrifluoromethane sulfonate

→

Methyl-Dithiane Triflate

반응 조건

후처리

1. 1
   기타After 20 minutes a white solid product was obtained in a salt form
2. 2
   여과The solid product was filtered
3. 3
   기타dried for 1 hour in an oven at 50° C.
4. 4
   기타to obtain the following product

실험 절차

2 mmol of 1,4-dithiane was dissolved in 8 ml of tetrahydrofuran at 0° C., and about 2 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture. After 20 minutes a white solid product was obtained in a salt form. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

출처