반응 #71571

반응 방정식

dimethyl sulfide

methyltrifluoromethane sulfonate

→

Trimethylsulfonium Triflate

용매

dichloromethane

반응 조건

후처리

1. 1
   기타to obtain a white solid product
2. 2
   여과The solid product was filtered
3. 3
   기타dried for 1 hour in an oven at 50° C.
4. 4
   기타to obtain the following product

실험 절차

16 mmol of dimethyl sulfide was dissolved in 10 ml of dichloromethane at 0° C., and about 17 mmol of methyltrifluoromethane sulfonate was slowly dripped to the mixture to obtain a white solid product. The solid product was filtered and dried for 1 hour in an oven at 50° C. to obtain the following product:

출처