반응 #71360

ord-52ef3b22410d44a3bc3e8ff2635df5e4

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The title compound was prepared in analogy to the procedure
  2. 2
    기타The latter compound was synthesized

실험 절차

The title compound was prepared in analogy to the procedure described in Step 14.1 but using 3-(4-ethylpiperazin-1-yl)-aniline (Step 2.1) and 8-isoquinolin-4-yl-quinoxaline-5-carboxylic acid. The latter compound was synthesized as described in Steps 1.2-1.7 but using 4-isoquinolineboronic acid in Step 1.4. Title compound: ESI-MS: 489.2 [M+H]+; tR=11.28 min (System 2).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08536175B2uspto-grants-2013_09