반응 #710460

반응 방정식

2-amino-3,5-dichlorobenzoic acid methyl ester

tert-butylamine

→

N-tert-butyl-2-amino-3,5-dichlorobenzamide

수율 90.4%

용매

methanol

반응 조건

후처리

1. 1
   workup.ADDITIONwere added
2. 2
   기타reacted for 5 hours

실험 절차

To a 100 mL round-bottom flask, 0.1 mol of 2-amino-3,5-dichlorobenzoic acid methyl ester having a structure as shown in VIII-1, 100 mL of methanol, and 0.4 mol of tert-butylamine were added, heated to 64° C. and reacted for 5 hours, after treatment 23.5 grams of N-tert-butyl-2-amino-3,5-dichlorobenzamide having a structural formula of III-1 was obtained, and the yield was 90.4%;

출처