반응 #710420

반응 방정식

thiophenol

→

phenylsulfide

용매

toluene

반응 조건

후처리

1. 1
   workup.ADDITIONwas treated with the procedure
2. 2
   기타The product was recrystallized from n-hexane

실험 절차

A mixture of bis(dineophyl-orthotrifluoromethylphenyltin)oxide (6.0 g, 5.6 mmol) prepared in Example 6, thiophenol (1.2 g, 11.2 mmol) and toluene (40 g) was treated with the procedure described in Example 7. The product was recrystallized from n-hexane to obtain 5.2 g of dineophylorthotrifluoromethylphenyltin phenylsulfide as a white solid.

출처