반응 #70846

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3-amino-5-methyl-2H-pyrazole

1-phenyl-2-(4-pyridyl)vinyl benzoate

1-Phenyl-2-(4-pyridyl)vinyl benzoate

→

title compound

수율 16.0%

4,6-Diphenyl-3-methyl-5-(4-pyridyl)-1H-pyrazolo[3,4-b]pyridine

수율 16.0%

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실험 절차

Following a similar procedure to that described in example 1 method B, but using 3-amino-5-methyl-2H-pyrazole instead of 3-amino-2H-pyrazole and 1-phenyl-2-(4-pyridyl)vinyl benzoate (obtained in reference example 5) instead of 1-(4-fluorophenyl)-2-(4-pyridyl)vinyl 4-fluorobenzoate, the title compound was obtained in solid white form (yield: 16%).

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