반응 #707873

반응 방정식

( D2.1 )

Methacrylate

TBAF

Irganox 1010

→

Allyl Methacrylate

용매

THF

반응 조건

후처리

1. 1
   온도The mixture warmed up
2. 2
   기타The last traces of THF were removed
3. 3
   온도by heating in a vacuum oven at 60° for 4 hours

실험 절차

To a stirred solution of MTS (5.5×10-3 g) in dry THF (10.0 ml) was added (D2.1) (3.0 g), AM (0.11 ml) and TBAF (2 μ1 of 1M THF solution). The mixture warmed up and was stirred overnight at room temperature. 50 ppm Irganox 1010 antioxidant was added to the very viscous clear solution, which was cast into a polyester tray in a stream of nitrogen. The last traces of THF were removed by heating in a vacuum oven at 60° for 4 hours.

출처