반응 #707641

ord-81048ea7faf3483092d2da47a242376d

반응 방정식

CC(C)C(O)C(C)(C)CO
2,2,4-trimethyl-1,3-dihydroxypentane
O=[N+]([O-])c1ccc(Cl)cc1
4-nitrochlorobenzene
[Na+].[OH-]
sodium hydroxide
→
CC(C)C(Oc1ccc([N+](=O)[O-])cc1)C(C)(C)COc1ccc([N+](=O)[O-])cc1
1,3-bis-(4-nitrophenoxy)-2,2,4-trimethylpentane

반응물

CC(C)C(O)C(C)(C)CO
2,2,4-trimethyl-1,3-dihydroxypentane
O=[N+]([O-])c1ccc(Cl)cc1
4-nitrochlorobenzene
[Na+].[OH-]
sodium hydroxide

시약

없음

용매

CS(C)=O
DMSO

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타were reacted

실험 절차

146 g (1 mol) 2,2,4-trimethyl-1,3-dihydroxypentane, 346.5 g (2.2 mols) 4-nitrochlorobenzene and 140 g powdered sodium hydroxide were reacted using the same procedure described in Example 1 in 600 ml DMSO.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04820866uspto-grants-1989_04