반응 #70344
ord-173a0ffe83b349cd963070606fb7fc29
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The solvent was evaporated
- 2기타the residue was triturated in diethyl ether
- 3기타The solid formed
- 4여과was filtered off
- 5기타to afford
실험 절차
A solution of 5-methyl-2-(6-morpholinopyridin-3-ylamino)benzoate tert-butyl ester in TFA (0.6 ml, 7.58 mmol) was stirred at room temperature for 1 hour. The solvent was evaporated and the residue was triturated in diethyl ether. The solid formed was filtered off to afford 0.047 g (73% of yield) of the expected product.