반응 #70287

반응 방정식

3-bromophenol

bromocyclopropane

K2CO3

Water

→

expected product

수율 83.1%

1-Bromo-3-cyclopropoxybenzene

수율 83.1%

용매

DMF

diethyl ether

반응 조건

후처리

1. 1
   기타the organic phase was evaporated

실험 절차

A mixture of 3-bromophenol (4.80 mmol, 0.83 g), bromocyclopropane (27.71 mmol, 2.22 ml), K2CO3 (23.15 mmol, 3.2 g) in DMF (18 ml) was heated at 180° C. for 8 hours in a microwave oven. Water and diethyl ether were added and the organic phase was evaporated affording 0.85 g of the expected product.

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