반응 #701472
ord-ad4528075d15412282c9ea1b8d0614a3
반응 방정식
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The product was recrystallized from ethanol
실험 절차
The procedures described above in Example 1 were carried out on 4.0 g. (0.0149 mole) of the product of Step A above and 2.68 g. (0.0149mole) of trisodiumphosphorothioate in 25 ml. of water. The product was recrystallized from ethanol: ether [m.p. 102-103° C. (decomposition)].