반응 #701472

ord-ad4528075d15412282c9ea1b8d0614a3

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The product was recrystallized from ethanol

실험 절차

The procedures described above in Example 1 were carried out on 4.0 g. (0.0149 mole) of the product of Step A above and 2.68 g. (0.0149mole) of trisodiumphosphorothioate in 25 ml. of water. The product was recrystallized from ethanol: ether [m.p. 102-103° C. (decomposition)].

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04144271uspto-grants-1979_03