반응 #70009

반응 방정식

hexafluoropropene

chloroform

→

CCl3CF2CHFCF3

반응 조건

후처리

1. 1
   온도The reactor pressure is maintained at 100 psig
2. 2
   workup.DISTILLATIONThe effluent from the reactor is fed into a distillation column
3. 3
   기타the unreacted reagents removed by distillation
4. 4
   기타The product CCl3CF2CHFCF3 is used in the next reaction

실험 절차

A 0.5 inch (12.7 mm) by 40 inch (101.6 cm) plug flow reactor that is packed with Helipack Monel support is heated to 290° C. A 50/50 (molar %) mixture of hexafluoropropene and chloroform is fed into the reactor at about 1.5 g/min. The reactor pressure is maintained at 100 psig. The effluent from the reactor is fed into a distillation column and the unreacted reagents removed by distillation and recycled. The product CCl3CF2CHFCF3 is used in the next reaction.

출처