반응 #694687

ord-b31f8f1e31714c4e87e66d77ec3f7303

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The procedure described in Example 2I was followed using a THF (30 ml) solution of 14A (5.92 g, 21.7 mmol), 2M sodium hydroxide aqueous solution (22 ml) and MeOH (30 ml) to give 5.0 g (94% yield) of the title compound as white solids.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07915448B2uspto-grants-2011_03