반응 #69039

반응 방정식

2-Phthalimidoethanesulfonyl chloride

methylamine

→

title compound

2-phthalimidoethane N-methylsulfonamide

용매

water

THF

반응 조건

후처리

1. 1
   기타the solution obtained this way

실험 절차

2-Phthalimidoethanesulfonyl chloride (2.0 g) was added portion wise to a solution of 2.0 M methylamine in THF (15 ml) and the solution obtained this way was stirred at room temperature. After 48 hours the reaction mixture was poured in water (50 ml) causing the title compound to precipitate. The product was collected by filtration and recrystallized from EtOH:water, 50:1 to yield: 1.04 g (48%) of the desired product as a solid.

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