반응 #69037

ord-e1c9c55b1bcd4e9bb9e477498827aec8

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Prepared

실험 절차

Prepared according to general method A from 2-phthalimidoethanesulfonyl chloride (1.50 g) and 4-iodoaniline (2.70 g). Yield: 1.56 g (56%). 1H-NMR (CDCl3) δ (ppm) 10.14 (s, 1H), 7.83 (s, 4H), 7.63 (d, J=8.7 Hz, 2H), 7.00 (d, J=8.8 Hz, 2H), 3.94 (t, J=7.1 Hz, 2H), 3.94-3.44 (m, 2H).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08530486B2uspto-grants-2013_09