반응 #681828

반응 방정식

benzo[b]thiophen-5-ylmethanamine

2,6-dimethoxybenzaldehyde

→

1-(benzo[b]thiophen-5-ylmethyl)-6-(2,6-dimethoxyphenyl)piperidin-2-one

반응 조건

후처리

1. 1
   기타Prepared
2. 2
   기타Subsequent purification by preparative HPLC
3. 3
   기타afforded the target compound

실험 절차

Prepared according to the described general procedure 6 (GP6) with commercially available benzo[b]thiophen-5-ylmethanamine and commercially available 2,6-dimethoxybenzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions E): tR=0.79 min.; [M+H]+: 382.09 g/mol.

출처