반응 #67854

반응 방정식

3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid

intermediate 2

3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid

O-methyl-hydroxylamine

→

N-methoxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide

반응 조건

후처리

1. 1
   기타LC/MS [8.75 min; 404 (M+1)]

실험 절차

N-methoxy-3-(2-chloro-4-iodo-phenylamino)-isonicotinamide was synthesized according to the procedure for General Method 1, outlined above, starting with 0.30 mmol of 3-[(2-chloro-4-iodophenyl)amino]isonicotinic acid (intermediate 2) and 0.42 mmol of O-methyl-hydroxylamine. LC/MS [8.75 min; 404 (M+1)]

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