반응 #67786
ord-eefb4f777a6c4d60abf2477d1e1f9e78
반응 조건
온도
75°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타The solvent was removed
실험 절차
To a solution of 3-fluoroisonicotinic acid (5.0 g, 35.33 mmol) in acetic acid (25 ml) was added hydrogen peroxide (6 ml). The reaction mixture was stirred at 70-80° C. overnight. The solvent was removed to obtain 5.5 g of 3-fluoroisonicotinic acid 1-oxide in quantitative yield.