반응 #671257
ord-f7c3e7476ee44cde8da15c899200e694
반응 방정식
5-bromo-2-chlorobenzotrifluoride
cis-2,6-dimethyl-1-propyl-piperazine
HCl
→
cis-4-(4-Chloro-3-trifluoromethyl-phenyl)-2,6-dimethyl-1-propyl-piperazine
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타the title compound was recovered by the procedure
- 2기타described in Preparation 9
실험 절차
Beginning with 5-bromo-2-chlorobenzotrifluoride and cis-2,6-dimethyl-1-propyl-piperazine, the title compound was recovered by the procedure described in Preparation 9: m.p. 256° C. (HCl), MS m/z (rel. intensity, 70 eV)) 335 (M+, 5), 305 (55), 112 (bp), 70 (67), 56 (82).