반응 #669980

ord-04bb0291bcd64345a483338c57e0abaa

반응 방정식

CCOC(CCO)OCC
3, 3-diethoxypropanol
[K].c1ccc2ccccc2c1
potassium naphthalene
[K]
potassium
CCOC(CCO)OCC
3, 3-diethoxypropanol

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

A reactor was charged with 30 ml of THF, 0.13 g of 3, 3-diethoxypropanol and 2 ml solution of potassium naphthalene dissolved in tetrahydrofuran in a concentration of 0.5 mol/L-tetrahydrofuran, and the resulting mixture was stirred for three minutes in an argon atmosphere, and, thus, there was formed a potassium derivative (potassium 3, 3-diethoxypropanoxide) of 3, 3-diethoxypropanol.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05925720uspto-grants-1999_07