반응 #66949

반응 방정식

3,4-Methylenedioxy-5-methoxybenzoic acid

thionyl chloride

→

3,4-methylenedioxy-5-methoxy-benzoyl chloride

용매

benzene

반응 조건

후처리

1. 1
   온도the resulting solution was refluxed for 15 hr
2. 2
   기타the solvent and excessive thionyl chloride were removed by distillation under reduced pressure

실험 절차

3,4-Methylenedioxy-5-methoxybenzoic acid (39.23 g, 0.2 mol) was dissolved in dry benzene, thionyl chloride 47.6 g (28.8 ml, 0.4 mol) was added under stirring, the resulting solution was refluxed for 15 hr, then the solvent and excessive thionyl chloride were removed by distillation under reduced pressure to give pure 3,4-methylenedioxy-5-methoxy-benzoyl chloride.

출처