반응 #667538
ord-7e5b6cf23b4a4a57b26e02bf28097737
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과The precipitated potassium chloride was filtered off
- 2농축the triphenyl methyl acrylate solution was concentrated by rotary evaporation at 65° to 100° C.
실험 절차
1 mole triphenylchloromethane was stirred with 1.5 moles potassium acrylate in 998 g dimethyl formamide in the presence of 0.14 g hydroquinone under the conditions described in Example 1. The precipitated potassium chloride was filtered off and the triphenyl methyl acrylate solution was concentrated by rotary evaporation at 65° to 100° C. and reduced to produce liquid triphenylmethyl acrylate. This was dissolved at 70 percent in xylene and filtered.