반응 #667243

반응 방정식

sodium hydride

2,4,6-trimethylphenol

3-tert-butyl-2-chloro-1,3,2-oxazaphospholidine

→

colorless liquid

수율 75.6%

3-tert-Butyl-2-(2,4,6-trimethylphenoxy)-1,3,2-oxazaphospholidine

수율 75.6%

용매

THF

THF

THF

반응 조건

실험 절차

The procedure of Example 1 is repeated using 4.4 g (0.11 mol) of sodium hydride with 45 ml of THF, 13.62 g (0.10 mol) of 2,4,6-trimethylphenol in 150 ml of THF and 18.16 g (0.10 mol) of 3-tert-butyl-2-chloro-1,3,2-oxazaphospholidine in 150 ml of THF to give a (75.6%) of colorless liquid: bp. 99°-103° C. (0.01 mm Hg).

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