반응 #66590

반응 방정식

Iodomethane

3-((dimethylamino)methyl)-5-methylhexan-2-one

→

title product

수율 68.4%

(2-Acetyl-4-methyl-pentyl)-trimethyl-ammonium iodide

수율 68.4%

용매

ethyl acetate

반응 조건

후처리

1. 1
   여과, and the resulting preciptant was collected by filtration

실험 절차

Iodomethane (20 g, 140.94 mmol, 2.00 equiv) was added dropwise to a solution of 3-((dimethylamino)methyl)-5-methylhexan-2-one (12 g, 70.05 mmol, 1.00 equiv) and ethyl acetate (50 mL). The solution was stirred at ambient temperature for about 16 hours., and the resulting preciptant was collected by filtration to afford the title product (15 g, yield=68%).

출처