반응 #663264

반응 방정식

Triphenylphosphine

(2-iodoethyl)cyclopropane

diethyl ether

→

(2-cyclopropylethyl)(triphenyl)phosphonium iodide

용매

acetonitrile

반응 조건

후처리

1. 1
   온도the mixture was heated
2. 2
   온도to reflux for 15 hr
3. 3
   온도After cooling
4. 4
   여과a precipitaed solid was collected by filtration

실험 절차

Triphenylphosphine (2.86 g, 10.9 mmol) was added to a solution of (2-iodoethyl)cyclopropane obtained (2.14 g, 10.9 mmol) in acetonitrile (5 mL), and the mixture was heated to reflux for 15 hr. After cooling, diethyl ether was added thereto and a precipitaed solid was collected by filtration to afford (2-cyclopropylethyl)(triphenyl)phosphonium iodide as a colorless powder (3.87 g).

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