반응 #66192

ord-30e92d70c0fe437cbd6454cf7b54316a

시약

없음

반응 조건

온도
20°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타Evaporation of solvent

실험 절차

To iso-propanol was added 3-bromopyruvic chloride (5 g) at −5° C. dropwise and the solution was stirred overnight at 20° C. Evaporation of solvent gave iso-propyl 3-bromopyruvate (3.5 g), which was used in the next step without further purification.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08524704B2uspto-grants-2013_09