반응 #66010

반응 방정식

allyl bromide

diethylene glycol

→

Diethylene glycol monoallyl ether

수율 82.0%

용매

THF NaH

반응 조건

후처리

1. 1
   기타The product was obtained in 82% yield
2. 2
   workup.DISTILLATIONafter distillation

실험 절차

Diethylene glycol monoallyl ether was prepared by reacting allyl bromide with excess diethylene glycol in THF-NaH (tetrahydrofuran-sodium hydride). The product was obtained in 82% yield after distillation. b.p.=96-99° C./7 mmHg.

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