반응 #658770

반응 방정식

9-phenylanthracene

bromosuccinimide

→

9-bromo-10-phenylanthracene

수율 89.3%

용매

N,N dimethylformamide

반응 조건

후처리

1. 1
   기타to react for six hours
2. 2
   workup.DISTILLATIONThen, distilled water
3. 3
   workup.ADDITIONwas added
4. 4
   기타the reaction
5. 5
   여과the deposit was filtered
6. 6
   기타The recovered deposit was purified by column chromatography

실험 절차

An amount of 13.65 (53.7 mmol) of 9-phenylanthracene was dissolved in 100 ml of N,N dimethylformamide. An amount of 10.5 g (59 mmol) of N bromosuccinimide was added and allowed to react for six hours. Then, distilled water was added to stop the reaction and the deposit was filtered. The recovered deposit was purified by column chromatography to obtain 15.97 g (48 mmol) of 9-bromo-10-phenylanthracene. The yield was 89.3%.

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