반응 #65834

반응 방정식

diisopropylethylamine

3-[3-(4-acetylphenylthio)phenyl]-3-methoxypyrrolidine

2-propynyl bromide

→

3-[3-(4-acetylphenylthio)phenyl]-3-methoxy-1-(prop-2-ynyl)pyrrolidine

수율 14.0%

반응 조건

실험 절차

Using an analogous procedure to that described in Example 3 except that diisopropylethylamine was used in place of potassium carbonate, 3-[3-(4-acetylphenylthio)phenyl]-3-methoxypyrrolidine was reacted with 2-propynyl bromide to give 3-[3-(4-acetylphenylthio)phenyl]-3-methoxy-1-(prop-2-ynyl)pyrrolidine as a gum in 14% yield.

출처