반응 #657262
ord-d4bd87fbd14f4d59b5abaf5b8b648ead
반응 방정식
ethyl 2-(bis(2-(3,5-bis(methoxymethyl)-1H-pyrazol-1-yl)ethyl)amino)acetate
LiAlH4
→
title compound
수율 60.0%
2-(bis(2-(3,5-bis(methoxymethyl)-1H-pyrazol-1-yl)ethyl)amino)ethanol
수율 60.0%
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타This compound has been obtained
실험 절차
This compound has been obtained by reacting a solution of ethyl 2-(bis(2-(3,5-bis(methoxymethyl)-1H-pyrazol-1-yl)ethyl)amino)acetate (280 mg; 0.6 mmol) in dry THF (10 mL) with LiAlH4. The title compound was isolated following the same methodology above described for the synthesis of other (hydroxymethyl)pyrazoles (see example 6). Yield: 60% (170 mg, 0.4 mmol).