반응 #6547

ord-9bcc3d835c564b278f0acc655903f697

반응 조건

온도
150°CELSIUS
상세 조건
See reaction.notes.procedure_details.

실험 절차

In a 100 ml autoclave were charged 13.7 g (0.201 mole) of cyclopentene, 24.8 g (0.183 mole) of trichlorosilane and 25 μl of a 0.077 m mole/ml chloroplatinic acid solution in isopropyl alcohol (platinum content 1.92×10-6 mole), which were then stirred at 150° C. for 30 minutes. Cyclopentyl trichlorosilane was obtained quantitatively.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05248803uspto-grants-1993_09