반응 #6545

ord-e4a11d3163094ac6b8aeb21c55a2d94d

반응 방정식

C1=CCCC1
cyclopentene
Cl[SiH](Cl)Cl
trichlorosilane
CC(C)O
isopropyl alcohol
Cl[Si](Cl)(Cl)C1CCCC1
Cyclopentyl trichlorosilane

반응 조건

온도
150°CELSIUS
상세 조건
See reaction.notes.procedure_details.

실험 절차

In a 100 ml autoclave were charged 13.9 g (0.204 mole) of cyclopentene, 25.1 g (0.185 mole) of trichlorosilane and 25 μl of a 0.077 m mole/ml chloroplatinic acid solution in isopropyl alcohol (platinum content 1.92×10-6 mole), which were then stirred at 150° C. for 30 minutes. Cyclopentyl trichlorosilane was obtained quantitatively.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05248803uspto-grants-1993_09