반응 #651857

ord-9577be13fb964738b2cfa0b4c31463a1

반응 방정식

CCCCCCOc1ccc2c(c1)CC(F)c1cc(OCCCCCC)ccc1-2
9-fluoro-2,7-dihexyloxy-9,10-dihydrophenanthrene
N#CC1=C(C#N)C(=O)C(Cl)=C(Cl)C1=O
DDQ
→
CCCCCCOc1ccc2c(c1)cc(F)c1cc(OCCCCCC)ccc12
9-Fluoro-2,7-dihexyloxyphenanthrene

반응물

CCCCCCOc1ccc2c(c1)CC(F)c1cc(OCCCCCC)ccc1-2
9-fluoro-2,7-dihexyloxy-9,10-dihydrophenanthrene
N#CC1=C(C#N)C(=O)C(Cl)=C(Cl)C1=O
DDQ

시약

없음

용매

Cc1ccccc1
toluene

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

From 9-fluoro-2,7-dihexyloxy-9,10-dihydrophenanthrene by dehydrogenation with DDQ in toluene.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06168838Auspto-grants-2001_01